Testing as an assessment technique has been widely used at all levels of education--from primary to higher school. The main purpose of the paper is to evaluate the effect of context-based testing in teaching and learning of analytical chemistry in a Russian university. The paper formulates the objectives of context-based testing, discusses its…

This experiment combines analytical techniques of solid phase microextraction and gas chromatography-mass spectrometry with easily relatable and accessible plant volatile chemistry (floral and vegetative scents of local/available plants). The biosynthesis and structure of these chemicals are of interest in the areas of organic chemistry,…

The derivation for the Gibbs phase rule, provided in physical chemistry text books, often assumes that all the components are present in all the phases coexisting at equilibrium. However, very often we have situations where all the phases at equilibrium do not have all the components, the binary eutectic system being a classic example. The melt…

Infrared (IR) spectroscopy is a vibrational spectroscopic technique useful in chemical, pharmaceutical, and forensic sciences. It is essential to identify chemicals for reasons spanning from scientific research and academic practices to quality control in companies. However, in some university degrees, graduate students do not get the proficiency…

The combination of organic synthesis and analytical chemistry into a related laboratory experiment is an excellent demonstration of the utility of making a compound to then be used further. Herein we describe an undergraduate laboratory experiment that involves the straightforward synthesis of an internal standard, ethyl 6-acetyloxyhexanoate, for…

This experiment combines analytical techniques of solid-phase extraction (SPE) and gas chromatography quadrupole time-of-flight mass spectrometry (GC-QTOF-MS) to determine organochlorine pesticides (OCPs) in river water as a means to develop and improve student understanding of the use of GC-QTOF-MS for qualitative and quantitative analysis. In…

Engaging undergraduates in the environmental consequences of fossil fuel usage primes them to consider their own anthropogenic impact, and the benefits and trade-offs of converting to renewable fuel strategies. This laboratory activity explores the potential contaminants (both inorganic and organic) present in the raw fuel and solid waste…

Undergraduate students in an environmental chemistry laboratory course were taught QuEChERS (quick, easy, cheap, effective, rugged, and safe), a sample preparation procedure that is commonly used in pesticide laboratories involving an acetonitrile salt-out extraction of fresh produce samples followed by solid-phase dispersive cleanup using a…

An experiment for the synthesis of N-acyl derivatives of natural amino acids has been developed as part of the Distributed Drug Discovery (D3) program. Students use solid-phase synthesis techniques to complete a three-step, combinatorial synthesis of six products, which are analyzed using LC-MS and NMR spectroscopy. This protocol is suitable for…

Describes Santa Fe Community College's Biological Parks Program for zookeepers, park naturalists, and animal technicians. Reveals that the program is meeting changing trends and current emphases of zoological organizations. Keynotes importance of technical writing skills and solid science background in chemistry and biology. (DMM)

Purpose: Municipal solid waste (MSW) consists mainly of several recyclable materials such as paper and cardboard. Inside the educational institutes, especially universities, MSW is generated from several facilities including offices and cafeterias. Without an effective management program, solid waste can have detrimental impacts on the…

We present the results of having applied a set of options in thermodynamics courses for encouraging a strong student in-class participation and engagement. Strong emphasis is given to planned ahead in-class student Q&As encompassing both thermodynamics and statistical mechanics and supplemented with take-home extra syllabus reading.…

Pigments, dyes, and transition-metal compounds are made in courses across the undergraduate chemistry curriculum, but student characterization of these compounds' most striking features, their colors, seldom goes beyond verbal descriptions. Affordable, hand-held, fiber-optic reflectance spectrophotometers make it possible to advance students'…

Anthocyanins are natural pigments belonging to the flavonoid family that generate the red, blue, and purple colors of fruits, vegetables, and flowers. Their structure and color are dependent on various factors, like the pH. Anthocyanins appear red in acidic, purple in neutral, and blue in basic solutions, making them suitable for use as natural pH…

A critical stage in the process of developing a conceptual understanding of organic chemistry is learning to use curved arrow notation. From this stems the ability to predict reaction products and mechanisms beyond the realm of memorization. Since evaluation (i.e., testing) is known to be a key driver of student learning, it follows that a new…