A Spreadsheet Excel application for chromatographic peak characterization is described in this article. Data are exported from HPLC specific program to an Excel file with macros to perform basic calculations as retention time, height, and area of the peaks. From these values, peak resolution, asymmetry, or theoretical plates are calculated and…

A multistep assembly of gold nanoparticle self-assembled monolayers (SAMs) on glass surfaces is proposed, as a third-year undergraduate experiment. The process includes self-assembly (SA) and electrostatic self-assembly (ESA) methods, which are central approaches in modern surface and materials engineering. The products are analyzed using…

Gamification of learning in chemistry education is a growing field. Chemistry themed escape room activities, incorporating course learning objectives into puzzle solution, have become a popular tool allowing for students to apply course knowledge in novel settings. Escape room activities, like their public counterparts, provide subtle guidance to…

A laboratory experiment in which [superscript 1]H NMR and UV-vis spectroscopies are applied to probe the temperature dependence of a monomer-dimer equilibrium involving a cyclopentadienone derivative is described and discussed. Details of the data analysis for extraction of equilibrium constants from the raw experimental data from both techniques…

The use of a multicompartment electrochemical cell for the potentiometric determination of solubility product constants of aqueous I[superscript -], Br[superscript -], SCN[superscript -], and Cl[superscript -] salts of silver is presented. An electrochemical cell presented in this study contained multiple half-cells made of disposable drinking…

The implementation of a laboratory exercise in an undergraduate chemistry course, where students perform a comparison of three different synthetic methods toward [Cu(Cl)(IPr)]-complexes (IPr = N,N'-bis(2,6-diisopropylphenyl)imidazol-2-ylidene), is described. The students are introduced to the continuous improvement of reactions in terms of green…

Within the past decade, escape rooms have aroused great social and educational interest. Their potential for intra- and extracurricular learning ranges from the promotion of methodical and communicative competencies to problem-solving and teamwork strategies. As a nonformal learning environment, the youth leisure sector is suitable for the…

An exciting recent development in chemistry has been the ability to control nanoparticle crystal morphology or shape. Nanoparticles of different shapes present different crystal surfaces (or facets) with respect to the surrounding environment. Synthetic control over nanoparticle morphology has enabled the study of the influence of surface facets…

This study aims to determine the need for multitiered diagnostic instruments to identify misconceptions and their causes, as well as multi-representational profiles in chemistry lessons starting from grade 10 in the initial to the final material for grade 12. The data analysis technique used in this research is descriptive, namely descriptive…

In this study, teaching materials related to the history of science (HOS) related to the Boyle-Hobbes debate were developed through the analytical lens of framing theory. Further, this study developed the teaching materials for learning the social-institutional aspects of the reconceptualized family resemblance approach (FRA) to the nature of…

The electrolysis of water to produce hydrogen is a critical step in many green chemistry processes. The key to the efficiency of water electrolysis is the synthesis of an appropriate electrocatalyst. Three-dimensional (3D) printing is an increasingly important part of many industrial processes. In this study, we propose an efficient laboratory…

A one-pot regio- and stereoselective synthesis of a dipyrromethane and a bis(indolyl)methane based on two consecutive reactions of nitrosoalkenes with pyrrole or indole, respectively, is described as an experiment to be carried out by upper-division undergraduate students in a laboratory classroom. Importantly, the ability of electrophilic…

This study is a follow up to two earlier studies characterizing student real-time use of mechanistic arrows. In these previous studies, students were asked to predict a product by drawing a curved arrow mechanism using an interface that allowed recording and replay of student actions. In the present study two different student cohorts responded to…

The amount of protein in complex matrices such as food products is an important characteristic, at both a nutritional and a pedagogical level. There are several methods available for protein quantification, from simple UV absorption to mass spectrometry. The most common are based on the interaction of the proteins with colored compounds followed…

The mercury beating heart is a classic demonstration to introduce redox reactions in the classroom. Here we report a new, safer demonstration: the Galinstan beating heart. Galinstan is a commercially available eutectic alloy composed of gallium (68.5%), indium (21.5%), and tin (10%) that has low toxicity. When an iron nail touches the Galinstan…