A detailed study of learning and teaching (L&T) of chemical engineering distillation to a mixed-ability small class of 13 students who are ordinarily full-time in-house employees in industry is reported. The course consisted of 9 × 2-h lectures (18 hours) and 9 × 2-h tutorials (18 hours). It was delivered over nine business days "in situ" in an established distillery. The purpose was to (re)learn core distillation of ethanol-water mixes at the level of higher education of a bachelor programme. There was 90% broad agreement that the course encouraged more learning. Students (40%) felt the course was too mathematical, however. Pointedly, there was good agreement (63%) that the course stimulated communication with each other professionally, and customers of the distillery. Results overall provide good evidence that students valued their L&T. The experimental design(s) could be readily applied to a range of fields of knowledge.